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Beilstein J. Org. Chem. 2018, 14, 1452–1458, doi:10.3762/bjoc.14.123
Graphical Abstract
Figure 1: Representative pharmaceutical agents bearing the CF3 group.
Figure 2: The structures of the Togni reagents 1-(trifluoromethyl)-1,2-benziodoxol-3(1H)-one (1) and trifluor...
Scheme 1: Our previous hypervalent iodine-mediated synthesis of 2H-azirine compounds.
Scheme 2: Study on the presumed Togni reagent 1-mediated trifluoromethylation followed by PhIO-mediated aziri...
Scheme 3: Togni reagent/PhIO-mediated one-pot synthesis of β-trifluoromethyl 2H-azirines. Reaction conditions...
Scheme 4: Control study with TEMPO.
Scheme 5: Proposed mechanism for the Togni reagent-mediated trifluoromethylation of enamines.